MIRAI MR99-K02 Bottle Sampling Water Chemical Analysis

Last Modified: 2017-07-28
: MR99-K02
: Processed (DMO)-QCed
: Temperature, Salinity, Dissolved oxygen, Chlorophyll, Silicate, Nitrate, Nitrite, Phosphate, Total inorganic carbon, Alkalinity, pH, Potential temperature, Density
:
OCEANS > OCEAN CHEMISTRY > INORGANIC CARBON
OCEANS > OCEAN CHEMISTRY > NITRITE
OCEANS > OCEAN CHEMISTRY > NITRATE
OCEANS > OCEAN CHEMISTRY > NUTRIENTS
OCEANS > OCEAN CHEMISTRY > OXYGEN
OCEANS > OCEAN CHEMISTRY > pH
OCEANS > OCEAN CHEMISTRY > PHOSPHATE
OCEANS > OCEAN CHEMISTRY > SILICATE
OCEANS > OCEAN CHEMISTRY > SALINITY
OCEANS > OCEAN CHEMISTRY > CHLOROPHYLL
OCEANS > OCEAN TEMPERATURE > WATER TEMPERATURE
OCEANS > SALINITY/DENSITY > SALINITY
OCEANS > OCEAN CHEMISTRY > ALKALINITY
OCEANS > OCEAN CHEMISTRY > CARBON
OCEANS > OCEAN TEMPERATURE > POTENTIAL TEMPERATURE

For Using Data

CTDTMP : Chizuru Saitoh (JAMSTEC)
CTDSAL : Chizuru Saitoh (JAMSTEC)
SALNTY : Chizuru Saitoh (JAMSTEC)
CTDOXY : Chizuru Saitoh (JAMSTEC)
OXYGEN : Chizuru Saitoh (JAMSTEC)
CHLORA : Kosei Sasaoka (Hokkaido University)
SILCAT : Chizuru Saitoh (JAMSTEC)
NITRAT : Chizuru Saitoh (JAMSTEC)
NITRIT : Chizuru Saitoh (JAMSTEC)
PHSPHT : Chizuru Saitoh (JAMSTEC)
TCARBN : Yuichiro Kumamoto (JAMSTEC)
ALKALI : Akihiko Murata (JAMSTEC)
PH : Andrey Andreev (JAMSTEC)
See Terms and Conditions about constrain of use.
See Terms and Conditions about data citation.
Instrument:
Salinity measurement system
Instrument:
Nutrient analyzer(4ch) ( - MR09-01)
Instrument:
Total dissolved inorganic carbon measurement system ( - MR11-E02)
Instrument:
pH meter ( - MR03-K04 Leg6)
Instrument:
Titrator for total alkalinity( - MR14-02)
Instrument:
Fluorometer (TURNER DESIGNS)
  • The values of nutrients (silicate, phosphate, and nitrate) have systematic errors among cruises, because the analytical methods used for these determinations, and the precision and standards for analysis varied slightly from cruise to cruise. The dataset posted here is "corrected" in a cruise. If you need the corrected data for systematic errors among cruises, please see "Hydrographic Data at Station K2 and KNOT". (Available data are station KNOT data only.)
  •  (1) Temperature sensor
         Model:               SBE3, Sea-Bird Electronics, Inc.
         Measurement range:   -5.0 to +35 deg C
         Accuracy:            0.001 deg C
         Resolution:          0.0002 deg C
     (2) Salinity sensor
         Model:               SBE4, Sea-Bird Electronics, Inc.
         Measurement range:   0.0 to 7 S/m
         Accuracy:            0.0003 S/m
         Resolution:          0.00004 S/m
     (3) Pressure sensor
         Model:               SBE9plus, Sea-Bird Electronics, Inc.
         Measurement range:   up to 10500 m
         Accuracy:            0.015% F.S.
         Resolution:          0.001% F.S.
     (4) DO sensor
         Model :               SBE13, Sea-Bird Electronics, Inc.
         Measurement range :   0-15ml/l(120% of surface saturation)
         Accuracy :            0.1ml/l(2% of saturation)
         Resolution :          0.01ml/l
    
        
         
     1. Dissolved Oxygen
     (1) Instruments: Titrator: Model 716 DMS Titrino (Metrohm)
                     Detector: Pt electrode
     (2) Methods:     Winkler method/potentiometric method
     (3) Precision:   0.44umol/kg
     (4) Reference Material/Calibration: 0.0100N KIO3 solution
     
    
     2. Salinity
     (1) Instruments: Autosal salinometer model 8400B (Guildline Instruments Ltd.)
     (2) Methods:     -
     (3) Precision:   -
     (4) Reference Material/Calibration: IAPSO Standard Sea Water batch P134 (Ocean Scientific International Ltd.)
     
    
     3. Silicate
     (1) Instruments: TRAACS800 (Bran+Luebbe)
     (2) Methods:     Molybdenum blue method
     (3) Precision:   From 0.03 to 2.6% except nitrite (CV%)
     (4) Reference Material/Calibration: -
     
    
     4. Nitrate
     (1) Instruments: TRAACS800 (Bran+Luebbe)
     (2) Methods:     Diazotization method (reduced to nitrite by Cd - Cu tube)
     (3) Precision:   From 0.03 to 2.6% except nitrite (CV%)
     (4) Reference Material/Calibration: -
     
    
     5. Nitrite
     (1) Instruments: TRAACS800 (Bran+Luebbe)
     (2) Methods:     Diazotization method
     (3) Precision:   -
     (4) Reference Material/Calibration: -
     
    
     6. Phosphate
     (1) Instruments: TRAACS800 (Bran+Luebbe)
     (2) Methods:     Molybdenum blue method
     (3) Precision:   From 0.03 to 2.6% except nitrite (CV%)
     (4) Reference Material/Calibration: -
     
    
     7. Total inorganic carbon
     (1) Instruments: automated TCO2 sampling system (Nippon ANS Inc.) equipped with carbon coulometer 5012 (UIC Inc.)
     (2) Methods:     coulometry
     (3) Precision:   less than 0.1%
     (4) Reference Material/Calibration: Na2CO3 solution and the CRM provided by Dr. Dickson in Scripps Institute of Oceanography
     
    
     8. Total Alkalinity
     (1) Instruments: auto-burette (Radiometer, ABU901), a pH glass electrode (Radiometer), a reference electrode (Radiometer)
     (2) Methods:     Modified Gran titration/Open-cell/potentiometry
     (3) Precision:   0.15% on average
     (4) Reference Material/Calibration: the CRM provided by Dr. Dickson in Scripps Institute of Oceanography
     
    
     9. pH
     (1) Instruments: a glass/reference electrode with a pH/Ion meter (Radiometer PHM95)
     (2) Methods:     potentiometric methods at 25deg-C
     (3) Precision:   -
     (4) Reference Material/Calibration: total hydrogen ion scale
     
    
     10. Chlorophyll-a
     (1) Instruments: Fluorophotometer model 10-AU (Turner design)
     (2) Methods:     extract in N,N-dimethylformamide/fluorometric determination (Parsons et al., 1984)
     (3) Precision:   -
     (4) Reference Material/Calibration: -
    
         
    : MR99-K02
    : Processed (DMO)-QCed
    : Temperature, Salinity, Dissolved oxygen, Chlorophyll, Silicate, Nitrate, Nitrite, Phosphate, Total inorganic carbon, Alkalinity, pH, Potential temperature, Density
    :
    OCEANS > OCEAN CHEMISTRY > INORGANIC CARBON
    OCEANS > OCEAN CHEMISTRY > NITRITE
    OCEANS > OCEAN CHEMISTRY > NITRATE
    OCEANS > OCEAN CHEMISTRY > NUTRIENTS
    OCEANS > OCEAN CHEMISTRY > OXYGEN
    OCEANS > OCEAN CHEMISTRY > pH
    OCEANS > OCEAN CHEMISTRY > PHOSPHATE
    OCEANS > OCEAN CHEMISTRY > SILICATE
    OCEANS > OCEAN CHEMISTRY > SALINITY
    OCEANS > OCEAN CHEMISTRY > CHLOROPHYLL
    OCEANS > OCEAN TEMPERATURE > WATER TEMPERATURE
    OCEANS > SALINITY/DENSITY > SALINITY
    OCEANS > OCEAN CHEMISTRY > ALKALINITY
    OCEANS > OCEAN CHEMISTRY > CARBON
    OCEANS > OCEAN TEMPERATURE > POTENTIAL TEMPERATURE

    Observation Map

    Imagery reproduced from ...

    Data List

    File names
    MR99K0200_ex_bot.csv
    MR99K0200_odv_bot.txt
    : MR99-K02
    : Processed (DMO)-QCed

    Exchange Format

    Provided in the Exchange Format of CCHDO (CLIVAR and Carbon Hydrographic Data Office).
    Please see the following link for details of Exchange Format.
    Format Information
    Column No. Column Heading Mnemonic Units Mnemonic Reporting Precision FORTRAN Format Comments
    1 EXPOCODE A14 Expedition code
    2 SECT A6 For WOCE data the WHP section identifier
    3 STNNBR A6 Station number
    4 CASTNO I3 Cast number
    5 SAMPNO A7 Sample number
    6 BTLNBR A7 Bottle identification number
    7 BTLNBR_FLAG_W I1 Bottle quality flag
    8 DATE I8 Cast date(UTC)
    9 TIME UTC I4 Cast time (UTC)
    10 LATITUDE DEG F8.3 LATITUDE
    11 LONGITUDE DEG F9.3 LONGITUDE
    12 DEPTH M I5 Reported depth to bottom.
    13 CTDPRS DBAR F9.1 Pressure
    14 CTDPRS_FLAG_W I1 Quality flag for CTD data
    15 CTDTMP ITS-90 F9.3 Temperature
    16 CTDTMP_FLAG_W I1 Quality flag for CTD data
    17 CTDSAL PSS-78 F9.3 CTD Salinity sensor
    18 CTDSAL_FLAG_W I1 Quality flag for CTD data
    19 SALNTY PSS-78 F9.3 Salinity
    20 SALNTY_FLAG_W I1 Quality flags for water samples
    21 CTDOXY ML/L F9.3 CTD Oxygen sensor
    22 CTDOXY_FLAG_W I1 Quality flag for CTD data
    23 OXYGEN UMOL/KG F9.1 Oxygen
    24 OXYGEN_FLAG_W I1 Quality flags for water samples
    25 CHLORA MG/CUM F9.3 Chlorophyll a
    26 CHLORA_FLAG_W I1 Quality flags for water samples
    27 SILCAT UMOL/KG F9.2 Silicate
    28 SILCAT_FLAG_W I1 Quality flags for water samples
    29 NITRAT UMOL/KG F9.2 Nitrate
    30 NITRAT_FLAG_W I1 Quality flags for water samples
    31 NITRIT UMOL/KG F9.2 Nitrite
    32 NITRIT_FLAG_W I1 Quality flags for water samples
    33 PHSPHT UMOL/KG F9.2 Phosphate
    34 PHSPHT_FLAG_W I1 Quality flags for water samples
    35 TCARBN UMOL/KG F9.1 Total carbon
    36 TCARBN_FLAG_W I1 Quality flags for water samples
    37 ALKALI UMOL/KG F9.1 Total alkalinity
    38 ALKALI_FLAG_W I1 Quality flags for water samples
    39 PH - F9.3 pH
    40 PH_FLAG_W I1 Quality flags for water samples
    41 THETA DEG C F9.3 Potential temperature
    42 SIG0 KG/CUM F9.3 Density

    ODV Format

    Please see the following link for details of ODV Format and ODV Software.
    Format Information
    Column No. Column Heading Comments
    1 Cruise Cruise Label
    2 Station Station number_Cast number
    3 Type Station type
    4 mon/day/yr Cast date(UTC)
    5 hh:mm Cast time (UTC)
    6 Latitude [degrees_north] LATITUDE
    7 Longitude [degrees_east] LONGITUDE
    8 Bot. Depth [m] Reported depth to bottom.
    9 CTDDPT[M] Depth(Calculate from CTDPRS and LATITUDE)
    10 QF Quality flag for CTD data
    11 CTDPRS[DBAR] Pressure
    12 QF Quality flag for CTD data
    13 CTDTMP[ITS-90] Temperature
    14 QF Quality flag for CTD data
    15 CTDSAL[PSS-78] CTD Salinity sensor
    16 QF Quality flag for CTD data
    17 SALNTY[PSS-78] Salinity
    18 QF Quality flags for water samples
    19 CTDOXY[ML/L] CTD Oxygen sensor
    20 QF Quality flag for CTD data
    21 OXYGEN[UMOL/KG] Oxygen
    22 QF Quality flags for water samples
    23 CHLORA[MG/CUM] Chlorophyll a
    24 QF Quality flags for water samples
    25 SILCAT[UMOL/KG] Silicate
    26 QF Quality flags for water samples
    27 NITRAT[UMOL/KG] Nitrate
    28 QF Quality flags for water samples
    29 NITRIT[UMOL/KG] Nitrite
    30 QF Quality flags for water samples
    31 PHSPHT[UMOL/KG] Phosphate
    32 QF Quality flags for water samples
    33 TCARBN[UMOL/KG] Total carbon
    34 QF Quality flags for water samples
    35 ALKALI[UMOL/KG] Total alkalinity
    36 QF Quality flags for water samples
    37 PH pH
    38 QF Quality flags for water samples
    39 THETA[DEG C] Potential temperature
    40 QF Quality flag for CTD data
    41 SIG0[KG/CUM] Density
    42 QF Quality flag for CTD data
    43 SAMPNO Sample number
    44 QF Bottle quality flag
    : MR99-K02
    : Processed (DMO)-QCed
    1. Quality control was carried out by ;
    2. DATA_ID Name
      CTDTMP JAMSTEC-DMO
      CTDSAL JAMSTEC-DMO
      SALNTY JAMSTEC-DMO
      CTDOXY JAMSTEC-DMO
      OXYGEN JAMSTEC-DMO
      CHLORA JAMSTEC-DMO
      SILCAT JAMSTEC-DMO
      NITRAT JAMSTEC-DMO
      NITRIT JAMSTEC-DMO
      PHSPHT JAMSTEC-DMO
      TCARBN JAMSTEC-DMO
      ALKALI JAMSTEC-DMO
      PH JAMSTEC-DMO
      PI : Quality control was carried out by PI (Principal Investigator)
      DMO : Quality control was carried out by JAMSTEC DMO

    3. Quality control in JAMSTEC DMO
    4. 1. Check of position/date/time/depth. (Compared with Cruise report or CTD cast table.)
      2. Flag and data check (Check the conformity of data with flag)
      3. Visual check of the Profiles. (If anomalous value is found, Questionable flag is added.)

    5. Quality flags
    6. Flags of data quality control are as follows.

    Related Information

    Update History

    2017-07-28
    An observation data was registerd.
    2015-05-29
    An observation data was registerd.
    2013-08-09
    An observation data was registerd.
    2013-01-25
    An observation data was registerd.