MIRAI MR11-05 Leg2 Bottle Sampling Water Chemical Analysis

Last Modified: 2018-01-25
: MR11-05 Leg2
: Processed (DMO/PI)
: JAMSTEC
: Temperature, Salinity, Dissolved oxygen, Fluorescence, Chlorophyll, PAR, Silicate, Nitrate, Nitrite, Phosphate, Ammonia, CFC11, CFC12, CFC113, Total inorganic carbon, Alkalinity, pH, DOC, Potential temperature, Density
:
OCEANS > OCEAN CHEMISTRY > AMMONIA
OCEANS > OCEAN CHEMISTRY > DISSOLVED GASES
OCEANS > OCEAN CHEMISTRY > INORGANIC CARBON
OCEANS > OCEAN CHEMISTRY > NITRITE
OCEANS > OCEAN CHEMISTRY > NITRATE
OCEANS > OCEAN CHEMISTRY > NUTRIENTS
OCEANS > OCEAN CHEMISTRY > OXYGEN
OCEANS > OCEAN CHEMISTRY > pH
OCEANS > OCEAN CHEMISTRY > PHOSPHATE
OCEANS > OCEAN CHEMISTRY > SILICATE
OCEANS > OCEAN CHEMISTRY > SALINITY
OCEANS > OCEAN CHEMISTRY > CHLOROPHYLL
OCEANS > OCEAN TEMPERATURE > WATER TEMPERATURE
OCEANS > SALINITY/DENSITY > SALINITY
OCEANS > OCEAN OPTICS > PHOTOSYNTHETICALLY ACTIVE RADIATION
OCEANS > OCEAN TEMPERATURE > SEA SURFACE TEMPERATURE
OCEANS > OCEAN CHEMISTRY > ALKALINITY
OCEANS > OCEAN CHEMISTRY > CARBON
OCEANS > OCEAN CHEMISTRY > OCEAN TRACERS
OCEANS > OCEAN OPTICS > FLUORESCENCE
OCEANS > OCEAN TEMPERATURE > POTENTIAL TEMPERATURE

For Using Data

CTDTMP : Masahide Wakita (JAMSTEC)
SBE35 : Masahide Wakita (JAMSTEC)
CTDSAL : Masahide Wakita (JAMSTEC)
SALNTY : Masahide Wakita (JAMSTEC)
CTDOXY : Masahide Wakita (JAMSTEC)
OXYGEN : Masahide Wakita (JAMSTEC)
OPTOXY : Masahide Wakita (JAMSTEC)
FLUOR : Masahide Wakita (JAMSTEC)
CHLORA : Kazuhiko Matsumoto (JAMSTEC)
CHLWELSH : Kazuhiko Matsumoto (JAMSTEC)
PAR : Masahide Wakita (JAMSTEC)
SILCAT : Michio Aoyama (Meteorological Research Institute)/Masahide Wakita (JAMSTEC)
NITRAT : Michio Aoyama (Meteorological Research Institute)/Masahide Wakita (JAMSTEC)
NITRIT : Michio Aoyama (Meteorological Research Institute)/Masahide Wakita (JAMSTEC)
PHSPHT : Michio Aoyama (Meteorological Research Institute)/Masahide Wakita (JAMSTEC)
NH4 : Michio Aoyama (Meteorological Research Institute)/Masahide Wakita (JAMSTEC)
CFCs : Ken-ichi Sasaki/Masahide Wakita (JAMSTEC)
TCARBN : Masahide Wakita (JAMSTEC)
ALKALI : Masahide Wakita (JAMSTEC)
PH : Masahide Wakita (JAMSTEC)
DOC : Masahide Wakita (JAMSTEC)
See Terms and Conditions about constrain of use.
See Terms and Conditions about data citation.
Instrument:
Gas chromatograph
Instrument:
Salinity measurement system
Instrument:
Nutrient analyzer(5ch) (MR09-02 - )
Instrument:
Total dissolved inorganic carbon measurement system (MR11-05 Leg1 - )
Instrument:
pH meter (MR02-K03 - )
Instrument:
Titrator for DO ( - MR11-05 Leg2)
Instrument:
Fluorometer (TURNER DESIGNS)
・Temperature data meserued by a mercury thermometer is listed in CTDTMP column at SAMPNO 0 which means sampled by bucket. Please notice that this data is different from other data in format (f9.1) and instrument.
・28 Feb. 2014 The data flag of MR110502_ex_bot.csv SALNTY are corrected. Because those data flag was used 0 instead of 2.
     
(1) Temperature sensor
    Model:               SBE03, Sea-Bird Electronics, Inc.
    Measurement range:   -5.0 to +35degC
    Accuracy:            0.001degC
    Resolution:          0.0002degC
    
(2) Salinity sensor
    Model:               SBE04, Sea-Bird Electronics, Inc.
    Measurement range:   0.0 to 7S/m
    Accuracy:            0.0003S/m
    Resolution:          0.00004S/m
    
(3) Pressure sensor
    Model:               SBE9plus, Sea-Bird Electronics, Inc.
    Measurement range:   up to 10500m
    Accuracy:            0.015%F.S.
    Resolution:          0.001%F.S.
    
(4) DO sensor
    Model:               SBE43, Sea-Bird Electronics, Inc.
    Measurement range:   120% of surface saturation
    Accuracy:            2% of saturation
    
(5) Optode oxygen sensor
    Model:               RINKO-III (JFE Advantech Co. Ltd.)
    Measurement range:   0 to 200%
    Accuracy:            ±2%F.S.
    Resolution:          0.01 to 0.04%
    
(6) Fluorometer
    Model:               (Seapoint Sensors, Inc.)
    Measurement range  : 0-5ug/l
    Resolution:          0.02ug/l
    
(7) Deep Ocean Standards Thermometer
    Model:               SBE 35, (Sea-Bird Electronics, Inc.)

(8) PAR sensor
    Model:               (Satlantic Inc.)   
     
1. Dissolved Oxygen 
(1) Instruments : 
                  Burette: APB-510 and APB-620 (Kyoto Electronic Co. Ltd.) / 10 cm3 of titration vessel
                  Detector : Automatic photometric titrator DOT-01 (Kimoto Electronic Co. Ltd)
                  Software : DOT controller Ver.2.2.1
(2)Methods:     Winkler method
(3)Precision:   Standard deviation 0.09 µmol kg-1 
(4)Reference Material/Calibration:  CSK standard of potassium iodate Lot EPJ3885 (Wako Pure Chemical Industries Ltd.,)0.0100N

2. Salinity 
(1)Instruments: Autosal salinometer model 8400B (Guildline Instruments Ltd.)
(2)Methods:     -
(3)Precision:   The average and standard deviation of absolute defference were 0.0002 and 0.0001 in salinity.
(4)Reference Material/Calibration: IAPSO Standard Sea Water batch P152 (Ocean Scientific International Ltd.)

3. Silicate
(1)Instruments: BL TEC K.K  QuAAtro 2-HR
(2)Methods:     Molybdenum blue method
(3)Precision:   C.V. 0.10%
(4)Reference Material/Calibration: RMNS, Silicon standard solution SiO2 in NaOH 0.5 mol/L CertiPUR® (Merck KGaA) 

4. Nitrate
(1)Instruments: BL TEC K.K  QuAAtro 2-HR
(2)Methods:     Diazotization method (reduced to nitrite by Cd - Cu tube)
(3)Precision:   C.V. 0.09%
(4)Reference Material/Calibration: RMNS, potassium nitrate 99.995 suprapur®  (Merck KGaA) 

5. Nitrite
(1)Instruments: BL TEC K.K  QuAAtro 2-HR
(2)Methods:     Diazotization method
(3)Precision:   C.V. 0.21%
(4)Reference Material/Calibration: RMNS, sodium nitrite (Wako Pure Chemical Industries, Ltd.)

6. Phosphate
(1)Instruments: BL TEC K.K  QuAAtro 2-HR
(2)Methods:     Molybdenum blue method
(3)Precision:   C.V. 0.18%
(4)Reference Material/Calibration: RMNS, potassium dihydrogen phosphate anhydrous 99.995 suprapur® (Merck KGaA)

7. Ammonia
(1)Instruments : BL TEC K.K  QuAAtro 2-HR
(2)Methods     : Indophenol method
(3)Precision   : C.V. 0.26%
(4)Reference Material/Calibration : ammonium sulfate (Wako Pure Chemical Industries, Ltd.)

8. Total inorganic carbon
(1)Instruments: TCO2 measuring system (Nippon ANS, Inc.) equipped with coulometer Model seacat2000(Nippon ANS, Inc.)
(2)Methods:     coulometry 
(3)Precision:   average of the differences 1.06umol kg-1, standard deviation 0.95umol kg-1
(4)Reference Material/Calibration: -

9. Total alkalinity
(1)Instruments: Spectrophotometric system(Nippon ANS, Inc.).
                The system comprises of a spectrophotometer (Carry 50 Scan, Varian)
(2)Methods:     Single step acid additional procedure/spectrophotometry
(3)Precision:   average of the differences 0.7umol kg-1, standard deviation 0.6umol kg-1
(4)Reference Material/Calibration: -

10. pH
(1)Instruments: pH/Ion meter Radiometer PHM240 (Radiometer Analytical SAS)
(2)Methods:     potentiometric methods
(3)Precision:   average 0.0001 pH unit, standard deviation 0.001 pH units 
(4)Reference Material/Calibration: total hydrogen ion scale

11. CFCs
(1)Instruments : Gas chromatograph (GC-14B: Shimadzu Ltd.)
(2)Methods     : see "Cruise report"
(3)Precision   : -
(4)Reference Material/Calibration : -

12. Chlorophyll a 
(1)Instruments : Fluorophotometer model 10-AU-005 (Turner design)
(2)Methods     : Extract in N,N-dimethylformamide / fluorometric determination (Non-acidification method and Acidification method)
(3)Precision   : -
(4)Reference Material/Calibration : -

13. DOC
(1)Instruments : Shimadzu TOC-V (Shimadzu Co.)
(2)Methods     : High temperature catalytic oxidation
(3)Precision   : -
(4)Reference Material/Calibration : -    
     
There are some description error for nutrient data of this cruise.
Please refer to the errata of the cruise report.
: MR11-05 Leg2
: Processed (DMO/PI)
: JAMSTEC
: Temperature, Salinity, Dissolved oxygen, Fluorescence, Chlorophyll, PAR, Silicate, Nitrate, Nitrite, Phosphate, Ammonia, CFC11, CFC12, CFC113, Total inorganic carbon, Alkalinity, pH, DOC, Potential temperature, Density
:
OCEANS > OCEAN CHEMISTRY > AMMONIA
OCEANS > OCEAN CHEMISTRY > DISSOLVED GASES
OCEANS > OCEAN CHEMISTRY > INORGANIC CARBON
OCEANS > OCEAN CHEMISTRY > NITRITE
OCEANS > OCEAN CHEMISTRY > NITRATE
OCEANS > OCEAN CHEMISTRY > NUTRIENTS
OCEANS > OCEAN CHEMISTRY > OXYGEN
OCEANS > OCEAN CHEMISTRY > pH
OCEANS > OCEAN CHEMISTRY > PHOSPHATE
OCEANS > OCEAN CHEMISTRY > SILICATE
OCEANS > OCEAN CHEMISTRY > SALINITY
OCEANS > OCEAN CHEMISTRY > CHLOROPHYLL
OCEANS > OCEAN TEMPERATURE > WATER TEMPERATURE
OCEANS > SALINITY/DENSITY > SALINITY
OCEANS > OCEAN OPTICS > PHOTOSYNTHETICALLY ACTIVE RADIATION
OCEANS > OCEAN TEMPERATURE > SEA SURFACE TEMPERATURE
OCEANS > OCEAN CHEMISTRY > ALKALINITY
OCEANS > OCEAN CHEMISTRY > CARBON
OCEANS > OCEAN CHEMISTRY > OCEAN TRACERS
OCEANS > OCEAN OPTICS > FLUORESCENCE
OCEANS > OCEAN TEMPERATURE > POTENTIAL TEMPERATURE

Observation Map

Imagery reproduced from ...

Data List

File names
MR110502_ex_bot.csv
MR110502_odv_bot.txt
: MR11-05 Leg2
: Processed (DMO/PI)
: JAMSTEC

Exchange Format

Provided in the Exchange Format of CCHDO (CLIVAR and Carbon Hydrographic Data Office).
Please see the following link for details of Exchange Format.
Format Information
Column No. Column Heading Mnemonic Units Mnemonic Reporting Precision FORTRAN Format Comments
1EXPOCODE
A14Expedition code
2SECT
A6For WOCE data the WHP section identifier
3STNNBR
A6Station number
4CASTNO
I3Cast number
5SAMPNO
A7Sample number
6BTLNBR
A7Bottle identification number
7BTLNBR_FLAG_W
I1Bottle quality flag
8DATE
I8Cast date(UTC)
9TIMEUTCI4Cast time (UTC)
10LATITUDEDEGF8.3LATITUDE
11LONGITUDEDEGF9.3LONGITUDE
12DEPTHMI5Reported depth to bottom.
13CTDDPTMF9.1Depth
14CTDDPT_FLAG_W
I1Quality flag for CTD data
15CTDPRSDBARF9.1Pressure
16CTDPRS_FLAG_W
I1Quality flag for CTD data
17CTDTMPITS-90F9.4Temperature
18CTDTMP_FLAG_W
I1Quality flag for CTD data
19SBE35ITS-90F10.5Temperature from Deep Ocean Standards Thermometer
20SBE35_FLAG_W
I1Quality flag for CTD data
21CTDSALPSS-78F9.4CTD Salinity sensor
22CTDSAL_FLAG_W
I1Quality flag for CTD data
23SALNTYPSS-78F9.4Salinity
24SALNTY_FLAG_W
I1Quality flags for water samples
25CTDOXYUMOL/KGF9.2CTD Oxygen sensor
26CTDOXY_FLAG_W
I1Quality flag for CTD data
27OPTOXYUMOL/KGF9.2Optode oxygen
28OPTOXY_FLAG_W
I1Quality flag for CTD data
29OXYGENUMOL/KGF9.2Oxygen
30OXYGEN_FLAG_W
I1Quality flags for water samples
31FLUORUG/LF9.3Fluorometer
32FLUOR_FLAG_W
I1Quality flag for CTD data
33CHLORAMG/CUMF9.2Chlorophyll a
34CHLORA_FLAG_W
I1Quality flags for water samples
35CHLWELSHMG/CUMF9.2Chlorophyll a (Welschmeyer method)
36CHLWELSH_W
I1Quality flags for water samples
37EDPARUMOL-PHOTONS/M2/SF9.3Ed PAR
38EDPAR_FLAG_W
I1Quality flag for CTD data
39SILCATUMOL/KGF9.2Silicate
40SILCAT_FLAG_W
I1Quality flags for water samples
41SILUNCUMOL/KGF9.2Uncertainty of Silicate data
42NITRATUMOL/KGF9.2Nitrate
43NITRAT_FLAG_W
I1Quality flags for water samples
44NRAUNCUMOL/KGF9.2Uncertainty of Nitrate data
45NITRITUMOL/KGF9.2Nitrite
46NITRIT_FLAG_W
I1Quality flags for water samples
47NRIUNCUMOL/KGF9.2Uncertainty of Nitrite data
48PHSPHTUMOL/KGF9.3Phosphate
49PHSPHT_FLAG_W
I1Quality flags for water samples
50PHPUNCUMOL/KGF9.3Uncertainty of Phosphate data
51NH4UMOL/KGF9.2Ammonium
52NH4_FLAG_W
I1Quality flags for water samples
53NH4UNCUMOL/KGF9.2Uncertainty of Ammonium data
54CFC-11PMOL/KGF9.3Freon-11
55CFC-11_FLAG_W
I1Quality flags for water samples
56CFC-12PMOL/KGF9.3Freon-12
57CFC-12_FLAG_W
I1Quality flags for water samples
58CFC113PMOL/KGF9.3Freon-113
59CFC113_FLAG_W
I1Quality flags for water samples
60TCARBNUMOL/KGF9.1Total carbon
61TCARBN_FLAG_W
I1Quality flags for water samples
62ALKALIUMOL/KGF9.1Total alkalinity
63ALKALI_FLAG_W
I1Quality flags for water samples
64PH-F9.3pH
65PH_FLAG_W
I1Quality flags for water samples
66DOCUMOL/KGF9.1Dissolved organic carbon
67DOC_FLAG_W
I1Quality flags for water samples
68THETADEG CF9.4Potential temperature
69SIG0KG/CUMF9.4Density

ODV Format

Please see the following link for details of ODV Format and ODV Software.
Format Information
Column No.Column HeadingComments
1CruiseCruise Label
2StationStation number_Cast number
3TypeStation type
4mon/day/yrCast date(UTC)
5hh:mmCast time (UTC)
6Latitude [degrees_north]LATITUDE
7Longitude [degrees_east]LONGITUDE
8Bot. Depth [m]Reported depth to bottom.
9CTDDPT[M]Depth
10QFQuality flag for CTD data
11CTDPRS[DBAR]Pressure
12QFQuality flag for CTD data
13CTDTMP[ITS-90]Temperature
14QFQuality flag for CTD data
15SBE35[ITS-90]Temperature from Deep Ocean Standards Thermometer
16QFQuality flag for CTD data
17CTDSAL[PSS-78]CTD Salinity sensor
18QFQuality flag for CTD data
19SALNTY[PSS-78]Salinity
20QFQuality flags for water samples
21CTDOXY[UMOL/KG]CTD Oxygen sensor
22QFQuality flag for CTD data
23OPTOXY[UMOL/KG]Optode oxygen
24QFQuality flag for CTD data
25OXYGEN[UMOL/KG]Oxygen
26QFQuality flags for water samples
27FLUOR[UG/L]Fluorometer
28QFQuality flag for CTD data
29CHLORA[MG/CUM]Chlorophyll a
30QFQuality flags for water samples
31CHLWELSH[MG/CUM]Chlorophyll a (Welschmeyer method)
32QFQuality flags for water samples
33EDPAR[UMOL-PHOTONS/M2/S]Ed PAR
34QFQuality flag for CTD data
35SILCAT[UMOL/KG]Silicate
36QFQuality flags for water samples
37SILUNCUncertainty of Silicate data
38QFQuality flags for water samples
39NITRAT[UMOL/KG]Nitrate
40QFQuality flags for water samples
41NRAUNCUncertainty of Nitrate data
42QFQuality flags for water samples
43NITRIT[UMOL/KG]Nitrite
44QFQuality flags for water samples
45NRIUNCUncertainty of Nitrite data
46QFQuality flags for water samples
47PHSPHT[UMOL/KG]Phosphate
48QFQuality flags for water samples
49PHPUNCUncertainty of Phosphate data
50QFQuality flags for water samples
51NH4[UMOL/KG]Ammonium
52QFQuality flags for water samples
53NH4UNCUncertainty of Ammonium data
54QFQuality flags for water samples
55CFC-11[PMOL/KG]Freon-11
56QFQuality flags for water samples
57CFC-12[PMOL/KG]Freon-12
58QFQuality flags for water samples
59CFC113[PMOL/KG]Freon-113
60QFQuality flags for water samples
61TCARBN[UMOL/KG]Total carbon
62QFQuality flags for water samples
63ALKALI[UMOL/KG]Total alkalinity
64QFQuality flags for water samples
65PHpH
66QFQuality flags for water samples
67DOC[UMOL/KG]Dissolved organic carbon
68QFQuality flags for water samples
69THETA[DEG C]Potential temperature
70QFQuality flag for CTD data
71SIG0[KG/CUM]Density
72QFQuality flag for CTD data
73SAMPNOSample number
74QFBottle quality flag
: MR11-05 Leg2
: Processed (DMO/PI)
: JAMSTEC
  1. Quality control was carried out by ;
  2. DATA_ID Name
    CTDTMPPI : Masahide Wakita (JAMSTEC)
    SBE35PI : Masahide Wakita (JAMSTEC)
    CTDSALPI : Masahide Wakita (JAMSTEC)
    SALNTYPI : Masahide Wakita (JAMSTEC)
    CTDOXYPI : Masahide Wakita (JAMSTEC)
    OXYGENPI : Masahide Wakita (JAMSTEC)
    OPTOXYPI : Masahide Wakita (JAMSTEC)
    FLUORJAMSTEC-DMO
    CHLORAPI : Kazuhiko Matsumoto (JAMSTEC)
    CHLWELSHPI : Kazuhiko Matsumoto (JAMSTEC)
    PARJAMSTEC-DMO
    SILCATPI : Michio Aoyama (Meteorological Research Institute)/Masahide Wakita (JAMSTEC)
    NITRATPI : Michio Aoyama (Meteorological Research Institute)/Masahide Wakita (JAMSTEC)
    NITRITPI : Michio Aoyama (Meteorological Research Institute)/Masahide Wakita (JAMSTEC)
    PHSPHTPI : Michio Aoyama (Meteorological Research Institute)/Masahide Wakita (JAMSTEC)
    NH4PI : Michio Aoyama (Meteorological Research Institute)/Masahide Wakita (JAMSTEC)
    CFCsPI : Ken-ichi Sasaki/Masahide Wakita (JAMSTEC)
    TCARBNPI : Masahide Wakita (JAMSTEC)
    ALKALIPI : Masahide Wakita (JAMSTEC)
    PHPI : Masahide Wakita (JAMSTEC)
    DOCPI : Masahide Wakita (JAMSTEC)
    PI : Quality control was carried out by PI (Principal Investigator)
    DMO : Quality control was carried out by JAMSTEC DMO
  3. Quality control in JAMSTEC DMO
  4. 1. Check of position/date/time/depth. (Compared with Cruise report or CTD cast table.)
    2. Flag and data check (Check the conformity of data with flag)
    3. Visual check of the Profiles. (If anomalous value is found, Questionable flag is added.)
  5. Quality flags
  6. Flags of data quality control are as follows.

Related Information

Update History

2018-01-25
An observation data was registerd.
2017-07-28
An observation data was registerd.
2015-05-29
An observation data was registerd.
2015-03-05
An observation data was registerd.
2014-09-03
An observation data was registerd.
2014-02-28
An observation data was registerd.
2013-09-12
An observation data was registerd.