MIRAI MR11-08 Leg3 Bottle Sampling Water Chemical Analysis

Last Modified: 2017-04-11
: MR11-08 Leg3
: Processed (PI)
: JAMSTEC
: Temperature, Salinity, Dissolved oxygen, Fluorescence, Chlorophyll, Transmittance, PAR, Density salinity, Silicate, Nitrate, Nitrite, Phosphate, CFC11, CFC12, CFC113, SF6, Total inorganic carbon, Alkalinity, pH, Carbon13, Carbon14, Tritium, 134Cs, 137Cs
:
OCEANS > OCEAN CHEMISTRY > DISSOLVED GASES
OCEANS > OCEAN CHEMISTRY > INORGANIC CARBON
OCEANS > OCEAN CHEMISTRY > NITRITE
OCEANS > OCEAN CHEMISTRY > NITRATE
OCEANS > OCEAN CHEMISTRY > NUTRIENTS
OCEANS > OCEAN CHEMISTRY > OXYGEN
OCEANS > OCEAN CHEMISTRY > pH
OCEANS > OCEAN CHEMISTRY > PHOSPHATE
OCEANS > OCEAN CHEMISTRY > RADIOCARBON
OCEANS > OCEAN CHEMISTRY > SILICATE
OCEANS > OCEAN CHEMISTRY > SALINITY
OCEANS > OCEAN CHEMISTRY > CHLOROPHYLL
OCEANS > OCEAN TEMPERATURE > WATER TEMPERATURE
OCEANS > SALINITY/DENSITY > SALINITY
OCEANS > OCEAN OPTICS > PHOTOSYNTHETICALLY ACTIVE RADIATION
OCEANS > OCEAN CHEMISTRY > ALKALINITY
OCEANS > OCEAN CHEMISTRY > CARBON
OCEANS > OCEAN CHEMISTRY > RADIONUCLIDES
OCEANS > OCEAN CHEMISTRY > OCEAN TRACERS
OCEANS > OCEAN OPTICS > FLUORESCENCE

For Using Data

CTDTMP : Hiroshi Uchida (JAMSTEC)
SBE35 : Hiroshi Uchida (JAMSTEC)
CTDSAL : Hiroshi Uchida (JAMSTEC)
SALNTY : Hiroshi Uchida (JAMSTEC)
CTDOXY : Hiroshi Uchida (JAMSTEC)
OXYGEN : Yuichiro Kumamoto (JAMSTEC)
FLUOR : Hiroshi Uchida (JAMSTEC)
XMISS : Hiroshi Uchida (JAMSTEC)
PAR : Hiroshi Uchida (JAMSTEC)
DNSSAL : Hiroshi Uchida (JAMSTEC)
CHLORA : Osamu Yoshida(Rakuno Gakuen University) /Hiroshi Uchida(JAMSTEC)
SILCAT : Michio Aoyama (Meteorological Research Institute)
NITRAT : Michio Aoyama (Meteorological Research Institute)
NITRIT : Michio Aoyama (Meteorological Research Institute)
PHSPHT : Michio Aoyama (Meteorological Research Institute)
CFCs : Kenichi Sasaki (JAMSTEC)
SF6 : Kenichi Sasaki (JAMSTEC)
TCARBN : Akihiko Murata (JAMSTEC)
ALKALI : Akihiko Murata (JAMSTEC)
PH : Akihiko Murata (JAMSTEC)
DELC14 : Yuichiro Kumamoto (JAMSTEC)
DELC13 : Yuichiro Kumamoto (JAMSTEC)
TRITUM : Yuichiro Kumamoto (JAMSTEC)/Tatsuo Aono(NIRS)
CS134 : Yuichiro Kumamoto (JAMSTEC)/Tatsuo Aono(NIRS)
CS137 : Yuichiro Kumamoto (JAMSTEC)/Tatsuo Aono(NIRS)
See Terms and Conditions about constrain of use.
See Terms and Conditions about data citation.
Instrument:
Salinity measurement system
Instrument:
Gas chromatograph
Instrument:
Nutrient analyzer(5ch) (MR09-02 - )
Instrument:
Total dissolved inorganic carbon measurement system (MR11-05 Leg1 - )
Instrument:
Titrator for DO Dissolved oxygen titration equipment (MR11-06 - )
Instrument:
Fluorometer (TURNER DESIGNS)
Parameters:CS-134, CS-137
Please cite the following paper.
Yuichiro Kumamoto, Michio Aoyama, Yasunori Hamajima, Akihiko Murata, Takeshi Kawano, Impact of Fukushima-derived radiocesium in the western North Pacific Ocean about ten months after the Fukushima Dai-ichi nuclear power plant accident, Journal of Environmental Radioactivity, Volume 140, 114–122 (2015), doi:10.1016/j.jenvrad.2014.11.010
Please see the Data book for details of data.
(1) Temperature sensor
    Model:               SBE03, Sea-Bird Electronics, Inc.
    Measurement range:   -5.0 to +35degC
    Accuracy:            0.001degC
    Resolution:          0.0002degC
    
(2) Salinity sensor
    Model:               SBE04, Sea-Bird Electronics, Inc.
    Measurement range:   0.0 to 7S/m
    Accuracy:            0.0003S/m
    Resolution:          0.00004S/m
    
(3) Pressure sensor
    Model:               SBE9plus, Sea-Bird Electronics, Inc.
    Measurement range:   up to 10500m
    Accuracy:            0.015%F.S.
    Resolution:          0.001%F.S.
    
(4) DO sensor
    Model:               RINKO-III (JFE Advantech Co. Ltd.)
    Measurement range:   0 to 200%
    Accuracy:            ±2%F.S.
    Resolution:          0.01 to 0.04%
    
(5) Fluorometer
    Model:               The Seapoint Chlorophyll Fluorometer (Seapoint Sensors, Inc.)
    Measurement range  : 0-5ug/l
    Resolution:          0.02ug/l
    
(6) Transmissometer
    Model :              C-Star WET Labs, Inc.
     
(7) Deep Ocean Standards Thermometer
    Model:               SBE 35, (Sea-Bird Electronics, Inc.)
    
(8) PAR sensor
    Model:               (Satlantic Inc.)    
     
1. Dissolved Oxygen 
(1)Instruments: 
                Burette : APB-620 and APB-510 (Kyoto Electronic Co. Ltd.) / 10 cm3 of titration vessel
                Detector : Automatic photometric titrator DOT-01X (Kimoto Electronic Co. Ltd)                  
(2)Methods:     Winkler method
(3)Precision:   Standard deviation of the replicate measurement  0.13 µmol kg-1
                Standard deviation of the duplicate measurement  0.14 µmol kg-1 
(4)Reference Material/Calibration:  CSK standard of potassium iodide Lot EPJ3885 (Wako Pure Chemical Industries Ltd.,)0.0100N

2. Salinity 
(1)Instruments: Autosal salinometer model 8400B (Guildline Instruments Ltd.)
(2)Methods:     -
(3)Precision:   The standard deviation of absolute defference were 0.00017
(4)Reference Material/Calibration: IAPSO Standard Sea Water batch P153

3. Silicate
(1)Instruments: BL TEC K.K  QuAAtro 2-HR
(2)Methods:     Molybdenum blue method
(3)Precision:   C.V. 0.14%
(4)Reference Material/Calibration: RMNS, Silicon standard solution SiO2 in NaOH 0.5 mol/L CertiPUR® (Merck KGaA) 

4. Nitrate
(1)Instruments: BL TEC K.K  QuAAtro 2-HR
(2)Methods:     Diazotization method (reduced to nitrite by Cd - Cu tube)
(3)Precision:   C.V. 0.12%
(4)Reference Material/Calibration: RMNS, potassium nitrate 99.995 Suprapur®  (Merck KGaA) 

5. Nitrite
(1)Instruments: BL TEC K.K  QuAAtro 2-HR
(2)Methods:     Diazotization method
(3)Precision:   -
(4)Reference Material/Calibration: RMNS, sodium nitrite (Wako Pure Chemical Industries, Ltd.)

6. Phosphate
(1)Instruments: BL TEC K.K  QuAAtro 2-HR
(2)Methods:     Molybdenum blue method
(3)Precision:   C.V. 0.20%
(4)Reference Material/Calibration: RMNS, potassium dihydrogen phosphate anhydrous 99.995 Suprapur® (Merck KGaA)

7. Total inorganic carbon
(1)Instruments: two TCO2 measuring system (Nippon ANS, Inc.)called as Systems C and D. The systems equipped with coulometer Model Seacat2000 and Model3000(Nippon ANS, Inc.)
(2)Methods:     coulometry 
(3)Precision:   Systems C 0.78±0.73µmol kg-1, Systems D 0.57±0.51µmol kg-1
(4)Reference Material/Calibration: -

8. Total alkalinity
(1)Instruments: Spectrophotometric systems(Nippon ANS, Inc.) .
                The system comprises of a spectrophotometer (Carry 50 Bio, Varian)
(2)Methods:     Single step acid additional procedure/spectrophotometry
(3)Precision:   0.51 ± 0.45 µmol kg-1
(4)Reference Material/Calibration: -

9. pH
(1)Instruments: pH measureing system (Nippon ANS, Inc.)
                The system comprises of a spectrophotometer (Carry 50 Scan, Varian)
(2)Methods:     potentiometric methods
(3)Precision:   The average of absolute differences 0.0007 ± 0.0006 pH unit 
(4)Reference Material/Calibration: -

10. CFCs
(1)Instruments : Gas chromatograph (GC-14B: Shimadzu Ltd.)
(2)Methods     : see "Cruise report"
(3)Precision   : CFC-11 ±0.005 pmol/kg,CFC-12 ±0.004 pmol/kg, CFC-113 ±0.003 pmol/kg
(4)Reference Material/Calibration : -

11. SF6
(1)Instruments : Gas chromatograph (GC-14B: Shimadzu Ltd.)
(2)Methods     : see "Cruise report"
(3)Precision   : ±0.03 fmol/kg
(4)Reference Material/Calibration : -

12. Chlorophyll a 
(1)Instruments : Fluorophotometer model 10-AU-005 (Turner design)
(2)Methods     : Extract in N,N-dimethylformamide / fluorometric determination (Non-acidification method)
(3)Precision   : -
(4)Reference Material/Calibration : Pure chlorophyll a (Sigma-Aldrich Co.)

13. DNSSAL
(1)Instruments : oscillation-type density meter DMA 5000M (Anton-Paar GmbH)
(2)Methods     : see "Cruise report"
(3)Precision   : -
(4)Reference Material/Calibration : -

14.δ13C and Δ14 C of Dissolved Inorganic Carbon
(1) Instruments:δ13C of the sample CO2 gas was measured using Finnigan MAT252 mass spectrometer.
                Δ14C in the graphite sample was measured in AMS facilities of Institute of Accelerator
                Analysis Ltd in Shirakawa (Pelletron 9SDH-2, NEC) and Paleo Labo Co. Ltd in Kiryu (Compact-AMS, NEC),Japan
(2) Methods    : 
(3) Precision  :"precisions" of our δ13C and Δ14C analyses including error due to the sample preparation and storage were about 0.03‰ and 6‰ respectively.
(4) Reference Material/Calibration: 

15. Tritium
(1) Instruments:mass spectrometer
(2) Methods    :the He-3 ingrowth method 
(3) Precision  : -
(4) Reference Material/Calibration: -

16. Cs-134 and Cs-137
(1) Instruments: low-background Ge-detectors, Well-type GCW2022-7915-30-ULB, Canberra Industries, Inc.
(2) Methods    : AMP treatment, gamma-ray analysis
(3) Precision  : -
(4) Reference Material/Calibration: -    
     
: MR11-08 Leg3
: Processed (PI)
: JAMSTEC
: Temperature, Salinity, Dissolved oxygen, Fluorescence, Chlorophyll, Transmittance, PAR, Density salinity, Silicate, Nitrate, Nitrite, Phosphate, CFC11, CFC12, CFC113, SF6, Total inorganic carbon, Alkalinity, pH, Carbon13, Carbon14, Tritium, 134Cs, 137Cs
:
OCEANS > OCEAN CHEMISTRY > DISSOLVED GASES
OCEANS > OCEAN CHEMISTRY > INORGANIC CARBON
OCEANS > OCEAN CHEMISTRY > NITRITE
OCEANS > OCEAN CHEMISTRY > NITRATE
OCEANS > OCEAN CHEMISTRY > NUTRIENTS
OCEANS > OCEAN CHEMISTRY > OXYGEN
OCEANS > OCEAN CHEMISTRY > pH
OCEANS > OCEAN CHEMISTRY > PHOSPHATE
OCEANS > OCEAN CHEMISTRY > RADIOCARBON
OCEANS > OCEAN CHEMISTRY > SILICATE
OCEANS > OCEAN CHEMISTRY > SALINITY
OCEANS > OCEAN CHEMISTRY > CHLOROPHYLL
OCEANS > OCEAN TEMPERATURE > WATER TEMPERATURE
OCEANS > SALINITY/DENSITY > SALINITY
OCEANS > OCEAN OPTICS > PHOTOSYNTHETICALLY ACTIVE RADIATION
OCEANS > OCEAN CHEMISTRY > ALKALINITY
OCEANS > OCEAN CHEMISTRY > CARBON
OCEANS > OCEAN CHEMISTRY > RADIONUCLIDES
OCEANS > OCEAN CHEMISTRY > OCEAN TRACERS
OCEANS > OCEAN OPTICS > FLUORESCENCE

Observation Map

Imagery reproduced from ...

Data List

  File names
49NZ20120113_hy1.csv
: MR11-08 Leg3
: Processed (PI)
: JAMSTEC

Exchange Format

Provided in the Exchange Format of CCHDO (CLIVAR and Carbon Hydrographic Data Office).
Please see the following link for details of Exchange Format.
Format Information
Column No. Column Heading Mnemonic Units Mnemonic Reporting Precision FORTRAN Format Comments
1EXPOCODE
A14Expedition code
2SECT_ID
A6For WOCE data the WHP section identifier
3STNNBR
A6Station number
4CASTNO
I3Cast number
5SAMPNO
A7Sample number
6BTLNBR
A7Bottle identification number
7BTLNBR_FLAG_W
I1Bottle quality flag
8DATE
I8Cast date(UTC)
9TIMEUTCI4Cast time (UTC)
10LATITUDEDEGF8.4LATITUDE
11LONGITUDEDEGF9.4LONGITUDE
12DEPTHMETERSI5Reported depth to bottom.
13CTDPRSDBARF9.1Pressure
14CTDPRS_FLAG_W
I1Quality flag for CTD data
15CTDTMPITS-90F9.4Temperature
16CTDTMP_FLAG_W
I1Quality flag for CTD data
17SBE35ITS-90F10.5Temperature from Deep Ocean Standards Thermometer
18SBE35_FLAG_W
I1Quality flag for CTD data
19CTDSALPSS-78F9.4CTD Salinity sensor
20CTDSAL_FLAG_W
I1Quality flag for CTD data
21SALNTYPSS-78F9.4Salinity
22SALNTY_FLAG_W
I1Quality flags for water samples
23DNSSALG/KGF9.4Quality-controlled density salinity data
24DNSSAL_FLAG_W
I1Quality flags for water samples
25CTDOXYUMOL/KGF9.2CTD Oxygen sensor
26CTDOXY_FLAG_W
I1Quality flag for CTD data
27OXYGENUMOL/KGF9.2Oxygen
28OXYGEN_FLAG_W
I1Quality flags for water samples
29XMISS%TRANSF9.3Transmissometer
30XMISSCP/METERF9.4Beam attenuation coefficient
31XMISS_FLAG_W
I1Quality flag for CTD data
32FLUORMG/CUMF9.3Fluorometer
33FLUOR_FLAG_W
I1Quality flag for CTD data
34CHLORAMG/CUMF9.2Chlorophyll a
35CHLORA_FLAG_W
I1Quality flags for water samples
36PARUE/SQM/SF9.3Ed PAR
37PAR_FLAG_W
I1Quality flag for CTD data
38SILCATUMOL/KGF9.2Silicate
39SILCAT_FLAG_W
I1Quality flags for water samples
40SILUNCUMOL/KGF9.2Uncertainty of Silicate data
41NITRATUMOL/KGF9.2Nitrate
42NITRAT_FLAG_W
I1Quality flags for water samples
43NRAUNCUMOL/KGF9.2Uncertainty of Nitrate data
44NITRITUMOL/KGF9.2Nitrite
45NITRIT_FLAG_W
I1Quality flags for water samples
46NRIUNCUMOL/KGF9.2Uncertainty of Nitrite data
47PHSPHTUMOL/KGF9.3Phosphate
48PHSPHT_FLAG_W
I1Quality flags for water samples
49PHPUNCUMOL/KGF9.3Uncertainty of Phosphate data
50CFC-11PMOL/KGF9.3Freon-11
51CFC-11_FLAG_W
I1Quality flags for water samples
52CFC-12PMOL/KGF9.3Freon-12
53CFC-12_FLAG_W
I1Quality flags for water samples
54CFC113PMOL/KGF9.3Freon-113
55CFC113_FLAG_W
I1Quality flags for water samples
56SF6FMOL/KGF9.3SF6
57SF6_FLAG_W
I1Quality flags for water samples
58TCARBNUMOL/KGF9.1Total carbon
59TCARBN_FLAG_W
I1Quality flags for water samples
60ALKALIUMOL/KGF9.1Total alkalinity
61ALKALI_FLAG_W
I1Quality flags for water samples
62PH_TOT
F9.4pH (Total scale)
63PH_TMPDEG CI9
Temperature of Analysis
64PH_TOT_FLAG_W
I1Quality flags for water samples
65DELC13/MILLEF9.313Carbon
66DELC13_FLAG_W
I1Quality flags for water samples
67C13ERR/MILLEF9.3Expected error
68DELC14/MILLEF9.114Carbon
69DELC14_FLAG_W
I1Quality flags for water samples
70C14ERR/MILLEF9.1Expected error
71TRITUMKBQ/CUMF9.3Tritium
72TRITUM_FLAG_W
I1Quality flags for water samples
73TRITERKBQ/CUMF9.3Expected error
74CS-134BQ/CUMF9.2134Cesium
75CS-134_FLAG_W
I1Quality flags for water samples
76CS134ERBQ/CUMF9.2Expected error
77CS-137BQ/CUMF9.2137Cesium
78CS-137_FLAG_W
I1Quality flags for water samples
79CS137ERBQ/CUMF9.2Expected error
: MR11-08 Leg3
: Processed (PI)
: JAMSTEC
  1. Quality control was carried out by ;
  2. DATA_ID Name
    CTDTMPPI : Hiroshi Uchida (JAMSTEC)
    SBE35PI : Hiroshi Uchida (JAMSTEC)
    CTDSALPI : Hiroshi Uchida (JAMSTEC)
    SALNTYPI : Hiroshi Uchida (JAMSTEC)
    CTDOXYPI : Hiroshi Uchida (JAMSTEC)
    OXYGENPI : Yuichiro Kumamoto (JAMSTEC)
    FLUORPI : Hiroshi Uchida (JAMSTEC)
    XMISSPI : Hiroshi Uchida (JAMSTEC)
    PARPI : Hiroshi Uchida (JAMSTEC)
    DNSSALPI : Hiroshi Uchida (JAMSTEC)
    CHLORAPI : Osamu Yoshida(Rakuno Gakuen University) /Hiroshi Uchida(JAMSTEC)
    SILCATPI : Michio Aoyama (Meteorological Research Institute)
    NITRATPI : Michio Aoyama (Meteorological Research Institute)
    NITRITPI : Michio Aoyama (Meteorological Research Institute)
    PHSPHTPI : Michio Aoyama (Meteorological Research Institute)
    CFCsPI : Kenichi Sasaki (JAMSTEC)
    SF6PI : Kenichi Sasaki (JAMSTEC)
    TCARBNPI : Akihiko Murata (JAMSTEC)
    ALKALIPI : Akihiko Murata (JAMSTEC)
    PHPI : Akihiko Murata (JAMSTEC)
    DELC14PI : Yuichiro Kumamoto (JAMSTEC)
    DELC13PI : Yuichiro Kumamoto (JAMSTEC)
    TRITUMPI : Yuichiro Kumamoto (JAMSTEC)/Tatsuo Aono(NIRS)
    CS134PI : Yuichiro Kumamoto (JAMSTEC)/Tatsuo Aono(NIRS)
    CS137PI : Yuichiro Kumamoto (JAMSTEC)/Tatsuo Aono(NIRS)
    PI : Quality control was carried out by PI (Principal Investigator)
    DMO : Quality control was carried out by JAMSTEC DMO
  • Quality control in JAMSTEC DMO
  • 1. Check of position/date/time/depth. (Compared with Cruise report or CTD cast table.)
    2. Flag and data check (Check the conformity of data with flag)
    3. Visual check of the Profiles. (If anomalous value is found, Questionable flag is added.)
  • Quality flags
  • Flags of data quality control are as follows. Quality flags

    Related Information

    Update History

    2017-04-11
    An observation data was registerd.
    2015-05-29
    An observation data was registerd.
    2015-02-05
    An observation data was registerd.
    2014-04-30
    An observation data was registerd.